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Reversed-phase high performance liquid chromatographic separation of the enantiomers of terbutaline by derivatization with 2,3,4,6-tetra-o-acetyl-β-D-glucopyranosyl isothiocyanate

✍ Scribed by Kyeong Ho Kim; Dong Sig Kim; Seon-Pyo Hong; Oh Seung Keon

Publisher
Springer
Year
2000
Tongue
English
Weight
312 KB
Volume
23
Category
Article
ISSN
0253-6269

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Reversed-phase liquid chromatographic re
Reversed-phase liquid chromatographic resolution of amino acid enantiomers by derivatization with 2,3,4,6-tetra-O-acetyl-β-d-glucopyranosyl isothiocyanate
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A novel method for reversed-phase high-performance liquid chromatographic resolution of amino acid enantiomers by the formation of diastereomers using 8 new chiral reagent, 2,3,4,6-tetra-O-acetyl+D-glucopyranosyl isothiocyanate (GITC), is described. GITC reacts readily with enantiomeric amino acids

Resolution of optical isomers of 2,3,4,6
Resolution of optical isomers of 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate (GITC)–derivatized DL-amino acids by micellar electrokinetic chromatography
✍ Hiroyuki Nishi; Tsukasa Fukuyama; Masaaki Matsuo 📂 Article 📅 1990 🏛 John Wiley and Sons 🌐 English ⚖ 475 KB

## Abstract Resolution of isomers of 2,3,4,6‐tetra‐__O__‐acetyl‐β‐D‐glucopyranosyl isothiocyanate (GITC)–derivatized DL‐amino acids was accomplished using micellar electrokinetic chromatography with sodium dodecyl sulfate (SDS) solutions. These solutes were not separated by the usual capillary zone