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Resolution of the enantiomers of thiol compounds by reversed-phase liquid chromatography using chiral derivatization with 2,3,4,6-tetra-O-acetyl-β-d-glucopyranosyl isothiocyanate

✍ Scribed by Susumu Ito; Atsutoshi Ota; Koji Yamamoto; Yoichi Kawashima

Publisher
Elsevier Science
Year
1992
Tongue
English
Weight
805 KB
Volume
626
Category
Article
ISSN
1873-3778

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Reversed-phase liquid chromatographic re
Reversed-phase liquid chromatographic resolution of amino acid enantiomers by derivatization with 2,3,4,6-tetra-O-acetyl-β-d-glucopyranosyl isothiocyanate
✍ Noriyuki Nimura; Haruo Ogura; Toshio Kinoshita 📂 Article 📅 1980 🏛 Elsevier Science 🌐 English ⚖ 359 KB

A novel method for reversed-phase high-performance liquid chromatographic resolution of amino acid enantiomers by the formation of diastereomers using 8 new chiral reagent, 2,3,4,6-tetra-O-acetyl+D-glucopyranosyl isothiocyanate (GITC), is described. GITC reacts readily with enantiomeric amino acids

Resolution of optical isomers of 2,3,4,6
Resolution of optical isomers of 2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl isothiocyanate (GITC)–derivatized DL-amino acids by micellar electrokinetic chromatography
✍ Hiroyuki Nishi; Tsukasa Fukuyama; Masaaki Matsuo 📂 Article 📅 1990 🏛 John Wiley and Sons 🌐 English ⚖ 475 KB

## Abstract Resolution of isomers of 2,3,4,6‐tetra‐__O__‐acetyl‐β‐D‐glucopyranosyl isothiocyanate (GITC)–derivatized DL‐amino acids was accomplished using micellar electrokinetic chromatography with sodium dodecyl sulfate (SDS) solutions. These solutes were not separated by the usual capillary zone