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Reinvestigation of the preparation of 131I-4-Iodoantipyrine from 131I-Iodide

โœ Scribed by G.D. Robinson Jr; A.W. Lee


Publisher
Elsevier Science
Year
1979
Weight
304 KB
Volume
30
Category
Article
ISSN
0020-708X

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๐Ÿ“œ SIMILAR VOLUMES


Preparation of no-carrier-added 4-[131i]
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The blood f l o w reagent 4-iodoantipyrine, l a b e l l e d w i t h 13'1 o r lZ5I, was prepared by a l l o w i n g aqueous a n t i p y r i n e t o r e a c t w i t h e i t h e r no-carrier-added 1311o r lZ5I-i n t h e presence o f c h l orami ne-T. P u r i f i c a t i o n o f 4-[ 13'I]i odoanti p y r

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The dried product (47 mg, m.p. 68-70ยฐ), homogeneous on t.l.c., was identified as 3,3-dimethylacrylic acid by comparison (i.r., n.m.r.) with an authentic sample. Spec. act. 3.1 x lo8 dpm/mmole. ## ACKNOWLEDGMENTS. We thank Mr. J. J. Ferrer for the i.r. and n.m.r. spectra, and the Consejo Nacional

Preparation of [131I] iodinated nonoxyno
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A novel method for the radioiodination [I3lI] of the multicomponent non-ionic surfactant nonoxynol-9 (N-9) is described. The extent of incorporation and distribution of the l31I-label into the aromatic moiety of various ethoxymer units of N-9 was determined utilizing a high pressure liquid chromatog