Single-crystal X-ray study T = 150 K Mean '(SeยฑGe) = 0.003 A ร R factor = 0.056 wR factor = 0.145 Data-to-parameter ratio = 15.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Reinvestigation of Ge4Se9 Based on Single-Crystal Data.
โ Scribed by Jung-Eun Kwak; Hoseop Yun
- Publisher
- John Wiley and Sons
- Year
- 2005
- Weight
- 9 KB
- Volume
- 36
- Category
- Article
- ISSN
- 0931-7597
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## Abstract The title compound with approximate composition Na~4~Ge~7.68~Si~1.32~O~20~ is hydrothermally prepared from a GeO~2~/xH~2~O/5en/2โmethyl pentanethylenediamine/yNaSiO~3~ยท9H~2~O (x = 35โ46; y = 0.1โ0.5) mixture (autoclave, 160 ยฐC, 7 d) and characterized by powder and single crystal XRD.