Reinvestigation of the Pb2[B5O9]Br structure based on single-crystal data
โ Scribed by Yakubovich, Olga V. ;Mochenova, Natalya N. ;Dimitrova, Olga. V. ;Massa, Werner
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 460 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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โฆ Synopsis
The structure of the title pentaborate, [Pb 2 (B 5 O 9 )Br] (dilead pentaborate bromide), known from powder data, has been reยฎned based on single-crystal data (R = 0.034) and is discussed in terms of intercrossing anionic and cationic frameworks.
๐ SIMILAR VOLUMES
Single-crystal X-ray study T = 150 K Mean '(SeยฑGe) = 0.003 A ร R factor = 0.056 wR factor = 0.145 Data-to-parameter ratio = 15.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The structure of trisodium phosphide, Na 3 P, known from X-ray powder diffraction data, has been refined based on single-crystal data. The compound crystallizes in the hexagonal A 3 B (A = alkali metal and B = group 15 element) structure type and is isotypic with the homologous potassium phase. The