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ChemInform Abstract: Si Modified Ge10 Cluster: The Preparation and Characterization of Single Crystal Na4(Ge,Si)9O20.

✍ Scribed by Peng-Yan Xiao; Tie-Zhen Ren; Zhi-Qiang Wang; K. E. Christensen

Publisher
John Wiley and Sons
Year
2010
Weight
18 KB
Volume
41
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

The title compound with approximate composition Na~4~Ge~7.68~Si~1.32~O~20~ is hydrothermally prepared from a GeO~2~/xH~2~O/5en/2‐methyl pentanethylenediamine/yNaSiO~3~Β·9H~2~O (x = 35β€”46; y = 0.1β€”0.5) mixture (autoclave, 160 Β°C, 7 d) and characterized by powder and single crystal XRD.

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Si modified Ge10 cluster: the preparatio
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Ge 10 cluster, Na 4 (Ge,Si) 9 O 20 , hydrothermal. A Si modified Ge 10 cluster with structure Na 4 (Ge,Si) 9 O 20 (denoted as HUT-1) was synthesized by hydrothermal synthesis at 160 Β°C with a sodium silicate source. The compound was characterized by single crystal, powder X-ray diffraction and TGA-

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