𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Reduction of disulfides in the milligram range with hypophosphorous acid and organic phosphites

✍ Scribed by R.E. Humphrey; C.L. Oleson; G.M. Matula; A.C. Vaught


Book ID
107828535
Publisher
Elsevier Science
Year
1971
Tongue
English
Weight
485 KB
Volume
16
Category
Article
ISSN
0026-265X

No coin nor oath required. For personal study only.


πŸ“œ SIMILAR VOLUMES


Selective synthesis of organic sulfides
✍ Akiya Ogawa; Noriaki Takami; Masahito Sekiguchi; Noboru Sonoda; Toshikazu Hirao πŸ“‚ Article πŸ“… 1998 πŸ› John Wiley and Sons 🌐 English βš– 128 KB πŸ‘ 2 views

Elemental sulfur can be reduced to the corresponding thiolate anion species (S β€«Χž2‬ and ) se- ## β€«Χž2‬ S 2 lectively by samarium diiodide in the presence and absence of HMPA, respectively. The subsequent alkylation of the thiolate anion species provides a useful synthetic route to dialkyl sulfides