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Redetermination of 1,3,6,8-tetraazatricyclo[4.4.1.1 3,8 ]dodecane

✍ Scribed by Rivera, Augusto; Ríos-Motta, Jaime; Bolte, Michael

Book ID
127263491
Publisher
International Union of Crystallography
Year
2014
Tongue
English
Weight
449 KB
Volume
70
Category
Article
ISSN
1600-5368

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An NMR study of sequential intermediates
An NMR study of sequential intermediates and collateral products in the conversion of 1,3,6,8-tetraazatricyclo[4.4.1.13,8]dodecane (TATD) to 1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecane (TATU)
✍ Augusto Rivera; Martín E. Núñez; Eliseo Avella; Jaime Ríos-Motta 📂 Article 📅 2008 🏛 Elsevier Science 🌐 French ⚖ 429 KB

In situ 1 H nuclear magnetic resonance spectroscopy was used to investigate the processes that occur during the synthesis of 1,3,6,8tetraazatricyclo[4.3.1.1 3,8 ]undecane (TATU). NMR analysis showed a reaction mixture containing more than one compound. The production of these intermediates and colla