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Electron Delocalization in the Radical Cation of 1,3,6,8-Tetraazatricyclo[4.4.1.1 3,8 ]dodecane, a 4-Nitrogen-7-Electron System

✍ Scribed by Zwier, Jurriaan M.; Brouwer, Albert M.; Keszthelyi, Tamás; Balakrishnan, Gurusamy; Offersgaard, Jesper F.; Wilbrandt, Robert; Barbosa, Frédérique; Buser, Urs; Amaudrut, Jérôme; Gescheidt, Georg; Nelsen, Stephen F.; Little, Charles D.

Book ID
120264525
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
265 KB
Volume
124
Category
Article
ISSN
0002-7863

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An NMR study of sequential intermediates
An NMR study of sequential intermediates and collateral products in the conversion of 1,3,6,8-tetraazatricyclo[4.4.1.13,8]dodecane (TATD) to 1,3,6,8-tetraazatricyclo[4.3.1.13,8]undecane (TATU)
✍ Augusto Rivera; Martín E. Núñez; Eliseo Avella; Jaime Ríos-Motta 📂 Article 📅 2008 🏛 Elsevier Science 🌐 French ⚖ 429 KB

In situ 1 H nuclear magnetic resonance spectroscopy was used to investigate the processes that occur during the synthesis of 1,3,6,8tetraazatricyclo[4.3.1.1 3,8 ]undecane (TATU). NMR analysis showed a reaction mixture containing more than one compound. The production of these intermediates and colla