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Three-electron .sigma. bonding in the radical cation from 1,3,6,8-tetraazatricyclo[4.4.1.13,8]dodecane

✍ Scribed by Nelsen, S. F.; Haselbach, E.; Gschwind, R.; Klemm, U.; Lanyova, S.


Book ID
120264518
Publisher
American Chemical Society
Year
1978
Tongue
English
Weight
255 KB
Volume
100
Category
Article
ISSN
0002-7863

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An NMR study of sequential intermediates
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In situ 1 H nuclear magnetic resonance spectroscopy was used to investigate the processes that occur during the synthesis of 1,3,6,8tetraazatricyclo[4.3.1.1 3,8 ]undecane (TATU). NMR analysis showed a reaction mixture containing more than one compound. The production of these intermediates and colla