𝔖 Bobbio Scriptorium
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Reciprocal biological activities of the cyclic tetrapeptides chlamydocin and HC-toxin

✍ Scribed by J. D. Walton; E. D. Earle; H. Stähelin; A. Grieder; A. Hirota; A. Suzuki

Book ID
105433362
Publisher
Springer
Year
1985
Tongue
English
Weight
365 KB
Volume
41
Category
Article
ISSN
1420-682X

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A novel double deprotection-peptide cycl
A novel double deprotection-peptide cyclisation procedure and its application to the synthesis of analogues of the cyclic tetrapeptide HC-toxin.
✍ Richard E Shute; Daniel H Rich 📂 Article 📅 1987 🏛 Elsevier Science 🌐 French ⚖ 318 KB

A hydroxide-mediated Fmoc/methyl ester double deprotection procedure followed by an improved bis(2-oxo-3-oxazolidinyl)phosphinic chloride (BOP-Cl) cyclisation reaction are reported. This novel methodology was applied to the synthesis of three new HC-toxin analogues.