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Reactions of 1,5-Dienes with Ruthenium Tetraoxide: Stereoselective Synthesis of Tetrahydrofurandiols

✍ Scribed by Laura Albarella; Domenica Musumeci; Donato Sica

Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
301 KB
Volume
2001
Category
Article
ISSN
1434-193X

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The N-substituted isomeric (4Z,5Z)-and (4E,5Z)-4,5-diethylideneoxazolidin-2-ones 5 and 6 were synthesized, the latter being favored during the one-step process from the a-diketone 1c and different isocyanates. The steric interaction between the N-substituent and the Me group attached to the exocycli