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Reaction of tungsten hexafluoride with Si and TiN surfaces

โœ Scribed by Michael J. Bozack

Publisher
Elsevier Science
Year
1992
Tongue
English
Weight
469 KB
Volume
221
Category
Article
ISSN
0040-6090

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Reaction of anionic and cationic silicon
Reaction of anionic and cationic silicon clusters with tungsten hexafluoride studied by fourier transform ion cyclotron resonance mass spectrometry
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Anionic and cationic silicon clusters react exothermically with WF6 to give a variety of tungsten and silicon fluorides. All the silicon anionic clusters transfer their charge to WF6. The electron affinities of S&, are estimated to be less than the electron affinity of WF6 (350 kJ/mole (3.6 eV)).

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Reaction of Tungsten Hexacarbonyl with Azide
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Tungsten hexacarbonyl reacts with alkali or tetraalkylammonium halides or pseudohalides MIX (X = halogen or NCS) with elimination of one CO ligand, giving compounds of the type MI[W(CO),X] 121. However, tetraethylammonium azide [31 and W(CO)6 (molar ratio 1 : 15) in diethylene glycol dimethyl ether