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Reaction of Activated Red Phosphorus with Phenylacetylene in the KOH-HMPA System

✍ Scribed by N. K. Gusarova; Yu. V. Smetannikov; B. G. Sukhov; S. F. Malysheva; N. P. Tarasova; B. A. Trofimov

Book ID
110312068
Publisher
Springer
Year
2001
Tongue
English
Weight
18 KB
Volume
71
Category
Article
ISSN
1070-3632

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## Abstract Red phosphorus reacts with 1‐bromonaphthalene in the KOH–DMSO system upon heating (47–70Β°C, 3 h) to give tri(1‐naphthyl)phosphane in 10% yield. Microwave activation (600 W, 6 min) of the reaction affords the above‐mentioned phosphane in 25% yield. Β© 2011 Wiley Periodicals, Inc. Heteroat