In the title compound, C 18 H 20 N 4 O 2 , the triazole ring is twisted with respect to the two benzene rings with dihedral angles of 71.5 (3) and 67.3 (3) . N-HÁ Á ÁN hydrogen bonding occurs between neighboring molecules.
✦ LIBER ✦
Reaction of 3-formyl-2-methoxy-1,6-dioxaspiro[4.4]nonanes with 3-amino-1,2,4-triazole: synthesis of 2-(1,2,4-triazolo[1,5-a]pyrimid-6-yl)methylenetetrahydrofurans
✍ Scribed by M. M. Vartanyan; O. L. Eliseev; T. Yu. Solov'eva; V. A. Petukhov
- Book ID
- 112387327
- Publisher
- Springer
- Year
- 1993
- Tongue
- English
- Weight
- 132 KB
- Volume
- 42
- Category
- Article
- ISSN
- 1573-9171
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## Abstract 5′‐Mercapto‐1′__H__‐1,2,4‐triazol‐3′‐yl‐isoquinolinium salts **(6)** were synthesised by the reaction of __ortho__‐acyl phenylacetones **(2)** or the corresponding pyrylium salts **(3)** and 5‐amino‐2,3‐dihydro‐1__H__‐1,2,4‐triazole‐3‐thione **(5)**. Treatment of thioles **6** withα,ω‐d