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Reaction of 1,3-Dialkyl-4,5-dimethylimidazol-2-ylidenes with 2-Bromo-2,3-dihydro-1H-1,3,2-diazaboroles (Alkyl=iPr andtBu)

✍ Scribed by Weber, Lothar ;Dobbert, Eckhard ;Stammler, Hans-Georg ;Neumann, Beate ;Boese, Roland ;Bläser, Dieter

Publisher
Wiley (John Wiley & Sons)
Year
1997
Tongue
English
Weight
631 KB
Volume
130
Category
Article
ISSN
0009-2940

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## Abstract 2,3‐Dihydro‐1,3‐diisopropyl‐4,5‐dimethylimidazol‐2‐ylidene **1** (Carb, R^1^ = ^i^Pr, R^2^ = Me) reacts with TeI~4~ to give the carbene adduct CarbTeI~2~ (**3**). The crystal structure of **3** consists of T‐shaped monomeric fragments linked by weak Te. I interactions to form infinite h

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1,3,2-diazaborole (4a) and Similarly, 1,3-di-tert-butyl-2-trimethylstannyl-2,3-dihydro-1H-1,3,2-diazaborole (8a) and 1,3-bis(2,6-dimethylphenyl)-2-1,3-bis(2,6-dimethylphenyl)-2,3-dihydro-1H-1,3,2-diazaborole (4b) were formed by the reaction of the corresponding trimethylstannyl-2,3-dihydro-1H-1,3,2-