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Pyrolysis of 1-(trimethylsilyl)-1-alkanols. New carbene precursors of silylcarbene and phenylcarbene

✍ Scribed by Sekiguchi, Akira; Ando, Wataru

Book ID: 127367761
Publisher: American Chemical Society
Year: 1980
Tongue: English
Weight: 629 KB
Volume: 45
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01314a012

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0.75 g, 15 mmol) and chlorotrimethylsilane (3.15 mL, 25 mmol) in dry acetonitrile (25 mL). The progress of the reactions was monitored by IR, and they were complete in 6-8 h. Pure silyl nitronates were obtained after workup and characterized by their NMR and IR spectra. Silyl nitronate of 6a: 1.0 g