Pulsed double resonance study of the 14N nuclear quadrupole coupling in glycine
✍ Scribed by R. Blinc; M. Mali; R. Osredkar; A. Prelesnik; I. Zupančič; L. Ehrenberg
- Publisher
- Elsevier Science
- Year
- 1971
- Tongue
- English
- Weight
- 237 KB
- Volume
- 9
- Category
- Article
- ISSN
- 0009-2614
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✦ Synopsis
The technique of nuclear magnetic pulsed double resonance in the rotating frame has been used to determine the quadrupole interactions of 14N in a single crystal of glycine nt 140°C. The 1% quldrupole coupling constant is found to be very small e%Q/fz = ;-%5kHz. whereas the ssymmetry paczmeter is relatively large ?J = 0.61. The direction of the Largest principal asis of the electric field gradient tensor does root coincide with the C-N direction as determined by X-ray data at room temperature.
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