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Process for the Capture and Reuse of the 4,4‘-Dimethoxytriphenylmethyl Group during Manufacturing of Oligonucleotides

✍ Scribed by Guo, Zhiqiang; Pfundheller, Henrik M.; Sanghvi, Yogesh S.

Book ID
125985692
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
69 KB
Volume
2
Category
Article
ISSN
1083-6160

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Analyses by flow injection as well as liquid chromatography/mass spectrometry (LC/MS) and liquid chromatography/tandem mass spectrometry (LC/MS/MS) were performed with four 4-phenoxyphenol derivatives. When ambient temperature nitrogen gas was used to facilitate solvent evaporation, [M + H]+, [M + N