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Preparation of tritiated water, sulfuric acid and trifluoroacetic acid

✍ Scribed by H. A. Dugger; H. J. Schwarz

Publisher
John Wiley and Sons
Year
1967
Tongue
French
Weight
302 KB
Volume
3
Category
Article
ISSN
0022-2135

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✦ Synopsis

A safe, eficient and inexpensive method for preparing small quantities of tritiated water, sulfuric acid and trifluoroacetic acid is described. The preparation involves introducing the preassayed tritium sample into a carrier gas, 0.5% hydrogen in air, passing over a palladium catalyst heated to 800Β° C. The resulting tritiated water is gradually eluted from the catalyst and collected in suitable traps.

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