Preparation of malvalic and sterculic acid methyl esters fromBombax mungubaandSterculia foetidaseed oils
✍ Scribed by E. Fehling; S. Schönwiese; E. Klein; K. D. Mukherjee; N. Weber
- Book ID
- 107496463
- Publisher
- Springer-Verlag
- Year
- 1998
- Tongue
- English
- Weight
- 72 KB
- Volume
- 75
- Category
- Article
- ISSN
- 0003-021X
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## Abstract Methyl esters were synthesized from lipid extracted by a modified __Bligh__ and __Dyer__ technique. The lipid was saponified and the free fatty acids methylated using boron trifluoride in methanol. Butylated hydroxytoluene (BHT; 2,6‐di‐__tert__‐butyl‐4‐methylphenol) was added to the ini
Fatty acids in oils were on-line methylated with acetyl chloride in methanol by dissotig 10-120 mg of oil in 100 ml of n-hexane, followed by continuous transesterification of the triglycerides, and flushing of residual reaction products by circulating a water stream through the derivatization manifo