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A Novel and Rapid Method for the Preparation of Methyl Esters for Gas Chromatography: Application to the Determination of the Fatty Acids of Edible Fats and Oils

✍ Scribed by McCreary, D. K.; Kossa, W. C.; Ramachandran, S.; Kurtz, R. R.


Book ID
126705131
Publisher
Preston Publications
Year
1978
Tongue
English
Weight
313 KB
Volume
16
Category
Article
ISSN
0021-9665

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Fatty acids in oils were on-line methylated with acetyl chloride in methanol by dissotig 10-120 mg of oil in 100 ml of n-hexane, followed by continuous transesterification of the triglycerides, and flushing of residual reaction products by circulating a water stream through the derivatization manifo