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Preparation of functionalized ketones via low temperature grignard reaction

✍ Scribed by Marcel K. Eberle; Gerard G. Kahle

Publisher: Elsevier Science
Year: 1980
Tongue: French
Weight: 118 KB
Volume: 21
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)92590-5

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✦ Synopsis

S-Chloroketones and 5-oxo-9-decenoic acid methyl ester were prepared from 5-chlorovaleryl chloride and methyl 4-(chloroformyl)-butyrate via Grignard reaction in tetrahydrofuran at -7OO.

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