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Preparation of [carboxy-13C]4-nitrophenylacetic acid

✍ Scribed by John E. T. Corrie; V. Ranjit N. Munasinghe

Book ID
102375128
Publisher
John Wiley and Sons
Year
2005
Tongue
French
Weight
74 KB
Volume
48
Category
Article
ISSN
0022-2135

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✦ Synopsis

Reaction of sodium [ 13 C]cyanide with excess benzyl chloride gave $75% utilization of the isotope. Subsequent nitration, isomer separation and hydrolysis of the nitrile gave the required carboxy-labelled 4-nitrophenylacetic acid.

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