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Preparation of allopregn-14-ene-3β, 20α-diol

✍ Scribed by F. S. Khristulas; M. B. Gorovits; N. K. Abubakirov

Book ID: 112375072
Publisher: Springer
Year: 1968
Tongue: English
Weight: 78 KB
Volume: 4
Category: Article
ISSN: 0009-3130
DOI: 10.1007/bf00568029

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## Abstract A convenient synthesis of 5α‐[20β‐^2^H]pregnane‐3α,20α‐diol and 5α‐[20β‐^2^H]pregnane‐3β,20α‐diol from 3β‐hydroxy‐5α‐pregn‐16‐en‐20‐one is described. The reaction products are characterized by combined gas chromatography‐mass spectrometry.