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Acid-Catalyzed Rearrangement of 20α-Ethynylpregn-5-ene-3β,20β-diol 3-Acetate 1

✍ Scribed by Chaudhuri, N. K.; Gut, Marcel

Book ID: 127323912
Publisher: American Chemical Society
Year: 1965
Tongue: English
Weight: 975 KB
Volume: 87
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01094a035

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## Abstract A convenient synthesis of 5α‐[20β‐^2^H]pregnane‐3α,20α‐diol and 5α‐[20β‐^2^H]pregnane‐3β,20α‐diol from 3β‐hydroxy‐5α‐pregn‐16‐en‐20‐one is described. The reaction products are characterized by combined gas chromatography‐mass spectrometry.