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Preparation of -(3S)-2,3-dimethylpentanal by reaction of (+)-tris[(2S)-1,2-dimethylbutoxy]methane (I) with carbon monoxide and hydrogen

✍ Scribed by Rossi, Renzo; Pino, Piero; Piacenti, Franco; Lardicci, Luciano; Del Bino, Goffredo

Book ID: 127125852
Publisher: American Chemical Society
Year: 1967
Tongue: English
Weight: 431 KB
Volume: 32
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo01278a084

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## The kinetics of the reaction of M O O S ~( S ~C N R ~) ~ ( R = C H ? , C2H,, n-C,H,) with PPh3 have been studied using a Stopped-flow method. It was found t h a t these M o O S ~~S ~C N R ~) ~ complexes react with PPh, in the form of an irreversible second-order reaction. The rate constants at