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Preparation of 3-amino-1,4-benzodiazepin-2-ones via direct azidation with trisyl azide

✍ Scribed by John W. Butcher; Nigel J. Liverton; Harold G. Selnick; Jason M. Elliot; Garry R. Smith; Andrew J. Tebben; David A. Pribush; John S. Wai; David A. Claremon

Book ID: 104255765
Publisher: Elsevier Science
Year: 1996
Tongue: French
Weight: 177 KB
Volume: 37
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(96)01475-x

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✦ Synopsis

An efficient synthesis of 3-amino-1,4-benzodiazepin-2-ones utilizing triisopropylbenzenesulfonyl azide (trisyl azide) for the direct azidation of 1,4-benzodiazepin-2-ones is described.

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