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ChemInform Abstract: Preparation of 3-Amino-1,4-benzodiazepin-2-ones via Direct Azidation with Trisyl Azide.

โœ Scribed by J. W. BUTCHER; N. J. LIVERTON; H. G. SELNICK; J. M. ELLIOT; G. R. SMITH; A. J. TEBBEN; D. A. PRIBUSH; J. S. WAI; D. A. CLAREMON

Book ID
112042082
Publisher
John Wiley and Sons
Year
2010
Weight
34 KB
Volume
27
Category
Article
ISSN
0931-7597

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Preparation of 3-amino-1,4-benzodiazepin
Preparation of 3-amino-1,4-benzodiazepin-2-ones via direct azidation with trisyl azide
โœ John W. Butcher; Nigel J. Liverton; Harold G. Selnick; Jason M. Elliot; Garry R. ๐Ÿ“‚ Article ๐Ÿ“… 1996 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 177 KB

An efficient synthesis of 3-amino-1,4-benzodiazepin-2-ones utilizing triisopropylbenzenesulfonyl azide (trisyl azide) for the direct azidation of 1,4-benzodiazepin-2-ones is described.