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Preparation of |2,4-2H|- and |2,4-3H|-tomatidine

✍ Scribed by D. Doller; E. G. Gros

Publisher
John Wiley and Sons
Year
1986
Tongue
French
Weight
179 KB
Volume
23
Category
Article
ISSN
0022-2135

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✦ Synopsis

2 3 The preparation of 12,4-HI-and 12,4-HI-tomatidine was accomplished by oxydation of the unlabelled compoun to tomatidone, exchange of and direct reduction of the labelled tomatidone to tomatidine. The efficiency of the procedure was checked by physical (1H and 33C NMR, MS) methods.

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