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Preparation of 15N labeled tetranitromethane C(15NO2)4

✍ Scribed by William Skawinski; Joseph Flisak; Alex C. Chung; Frank Jordan; Richard Mendelsohn

Publisher
John Wiley and Sons
Year
1990
Tongue
French
Weight
211 KB
Volume
28
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

^15^N labeled tetranitromethane, C(^15^NO~2~)~4~, was prepared from anhydrous nitric acid and acetic anhydride. A procedure for the preparation of the nitric acid from Na^15^NO~3~ is described. Tyrosine was nitrated with H^15^NO~3~ and its ^15^N NMR spectrum compared well with that of tyrosine nitrated with C(^15^NO~2~)~4~.

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