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ChemInform Abstract: High-Yielding Preparation of [3-15N]Cytidine, [4-15NH2]Cytidine, and [3-15N,4-15NH2]Cytidine.

✍ Scribed by Xavier Ariza; Jaume Vilarrasa

Publisher
John Wiley and Sons
Year
2010
Weight
26 KB
Volume
31
Category
Article
ISSN
0931-7597

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The 15N NMR spectra of the novel seven-membered 1,2,3,5-tetrazepinone ring systems were studied. The chemical shift of N-2 was found to be signiÐcantly responsive to substituent changes at the phenyl ring. As the electron-withdrawing character of the substituents increased, N-2 became more deshielde