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Preparation of 1-Alkyluramil-7,7-diacetic Acids

✍ Scribed by Stein, Alvin; Gregor, Harry P.; Spoerri, Paul E.

Book ID
119992457
Publisher
American Chemical Society
Year
1956
Tongue
English
Weight
523 KB
Volume
78
Category
Article
ISSN
0002-7863

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Preparation of [7,7-2H2] lithocholic aci
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✍ G. Phillipou; C. J. Seaborn; R. N. Butler πŸ“‚ Article πŸ“… 1981 πŸ› John Wiley and Sons 🌐 French βš– 206 KB

## Abstract Electrochemical deoxygenation of methyl 7‐keto‐lithocholate using deuterated reagents, followed by base hydrolysis is shown to give [7,7‐^2^H~2~] lithocholic acid in 60% overall yield and 86% ^2^H~2~ isotopic purity.