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Preparation and electrochemistry of thiolate-phosphine complexes of osmium

✍ Scribed by Marie-Laurence Abasq; Christopher J. Pickett; Raymond L. Richards; Maribel Arroyo; José A. Chamizo; Antonio Calderon; Plinio Sosa; Hugo Torrens

Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
455 KB
Volume
15
Category
Article
ISSN
0277-5387

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Addition of (Bu4N) [TcOC14] to a stirred solution of the acetamidomethylprotected ligand 1 at room temperature gives immediate formation of the neutral complex 8 which has been spectroscopically and structurally characterized. An ORTEP drawing of 8 is shown in Figure 2 (cell data are a=8.010(2)& b=8