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Sulfur protecting groups in the preparation of technetium(V) thiolate complexes

✍ Scribed by A. Davison; J. Lister-James; N. Brvson; A.G. Jones

Publisher
John Wiley and Sons
Year
1989
Tongue
French
Weight
76 KB
Volume
26
Category
Article
ISSN
0022-2135

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✦ Synopsis

Addition of (Bu4N) [TcOC14] to a stirred solution of the acetamidomethylprotected ligand 1 at room temperature gives immediate formation of the neutral complex 8 which has been spectroscopically and structurally characterized. An ORTEP drawing of 8 is shown in Figure 2 (cell data are a=8.010(2)& b=8.010(2) A, c=36.845(7)& p=94.29( l)', space group=P43212, 2=8,

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