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Practical synthesis of deuterium-labeled methyl sulfide, methyl disulfide, methanethiol, and methanesulfenyl compounds

✍ Scribed by Kim, Jhong K.; Lingman, Eric; Caserio, Marjorie C.


Book ID
126236847
Publisher
American Chemical Society
Year
1978
Tongue
English
Weight
310 KB
Volume
43
Category
Article
ISSN
0022-3263

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Synthesis of deuterium-labeled (24R)-met
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## Abstract Synthesis of labeled brassinosteroids (24‐epibrassinolide and its biosynthetic precursors) containing three deuterium atoms in the terminal part of the side chain is reported. Labeling was achieved by three‐step reductive transformation of carbethoxy group into methyl using lithium alum