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Practical Biostatistics || Step 2: n Estimation and n Assessment of a Published Trial

✍ Scribed by Suchmacher, Mendel

Book ID
120468969
Publisher
Elsevier
Year
2012
Weight
524 KB
Category
Article
ISBN
0124157947

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The resolution of (\_+)-2-methylpiperidine using D-and L-tartaric acid followed by direct conversion of the intermediate tartrate salts to (R) and (S)-N-Boc-2methylpiperidine is described. Also described is an NMR protocol for assessing the optical purity of the intermediate tartrate salts as well a