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Plate-to-Plate Fluorous Solid-Phase Extraction for Solution-Phase Parallel Synthesis

✍ Scribed by Zhang, Wei; Lu, Yimin; Nagashima, Tadamichi

Book ID
126818566
Publisher
American Chemical Society
Year
2005
Tongue
English
Weight
107 KB
Volume
7
Category
Article
ISSN
1520-4766

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πŸ“œ SIMILAR VOLUMES

Fluorous electrophilic scavengers for so
Fluorous electrophilic scavengers for solution-phase parallel synthesis
✍ Wei Zhang; Christine Hiu-Tung Chen; Tadamichi Nagashima πŸ“‚ Article πŸ“… 2003 πŸ› Elsevier Science 🌐 French βš– 341 KB

A fluorous isatoic anhydride and isocyanate are synthesized and used as scavengers for amines in solution-phase parallel synthesis of urea, thiourea, and b-hydroxyamine analogs. The resulting fluorous derivatives are readily separated from the reaction mixture by solid-phase extractions (SPE) over F

Fluorous-tethered quenching reagents for
Fluorous-tethered quenching reagents for solution phase parallel synthesis
✍ Craig W. Lindsley; Zhijian Zhao; William H. Leister πŸ“‚ Article πŸ“… 2002 πŸ› Elsevier Science 🌐 French βš– 124 KB

Commercially available fluorous-tethered reagents are employed to quench excess reactants and remove known impurities from crude reaction mixtures generated via solution phase parallel synthesis. Fluorous quenching reagents are expediently removed via FluoroFlashβ„’ SPE columns to afford products in h