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Piperazinium dihydrogen phosphate, C4H12N2(H2PO4)2: Synthesis, 31P CP/MAS NMR, structural and thermal investigations

✍ Scribed by Torben R. Jensen; Jens-Erik Jørgensen; Rita G. Hazell; Hans J. Jakobsen; Marie-Agnes Chevallier; Lene Jørgensen; Aleksandra Wiedermann


Book ID
113913201
Publisher
Elsevier Science
Year
2007
Tongue
English
Weight
691 KB
Volume
9
Category
Article
ISSN
1293-2558

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Hydrothermal Synthesis and Characterizat
✍ Junghwan Do; Ranko P. Bontchev; Allan J. Jacobson 📂 Article 📅 2000 🏛 Elsevier Science 🌐 English ⚖ 488 KB

Two new phases, (C 4 H 12 N 2 )(H 3 O)[(VOPO 4 ) 4 (H 2 O)H 2 PO 4 ] ' 3H 2 O (1) and (C 4 H 12 N 2 )[(VO)(VO 2 ) 2 (H 2 O)(PO 4 ) 2 ] (2) have been synthesized hydrothermally and characterized by single crystal X-ray di4raction, thermogravimetric analysis, and magnetic susceptibility. Compound 1 ha