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Photodimerization of dibenz[b,f] azepine derivatives and their reaction intermediates

✍ Scribed by Kazuo Ashikaga; Shinzaburo Ito; Masahide Yamamoto; Yasunori Nishijima

Publisher
Elsevier Science
Year
1987
Weight
605 KB
Volume
38
Category
Article
ISSN
0047-2670

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Reactions of 5-carboxamido-5H-dibenz[bflazepines (la-ld) with glyoxylic acid methylester methyl hemiacetal (GMHA) led to 5-(carboxamido-N-a-hydroxy-acetic acid methyl ester)-5Hdibenz[b,Aazepines (2a-2d). The reactions with glycols yielded the oligoethylene glycol derivatives (3,4). The new compounds