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Phenylbis[3,5-bis(trifluormethyl)-1,2,4-triazol-1-yl]methan

✍ Scribed by Gieren, A. ;Riemann, U.


Book ID
114526670
Publisher
International Union of Crystallography
Year
1980
Weight
447 KB
Volume
36
Category
Article
ISSN
0567-7408

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Bis­[4-phenyl-5-(1H-1,2,4-triazol-3-yl)-
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The title compound, C 20 H 14 N 12 S 2 , was synthesized by the reaction of 3-hydrazino-1H-1,2,4-triazole with phenyl isocyanate in benzene and by ring closure in an alkaline medium. Intermolecular N-HÁ Á ÁN hydrogen bonds are observed and these form a five-membered ring.

1-Amino-2,5-bis­(4-methoxy­benz­yl)-1,3,
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In the title compound, C 18 H 20 N 4 O 2 , the triazole ring is twisted with respect to the two benzene rings with dihedral angles of 71.5 (3) and 67.3 (3) . N-HÁ Á ÁN hydrogen bonding occurs between neighboring molecules.