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(Ph4P)S6—A Compound Containing the Cyclic Radical Anion S6.−

✍ Scribed by Bernhard Neumüller; Fritjof Schmock; Reinhard Kirmse; Andreas Voigt; Axel Diefenbach; F. Matthias Bickelhaupt; Kurt Dehnicke

Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
104 KB
Volume
39
Category
Article
ISSN
0044-8249

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The reaction of one equivalent of In with a molten flux of (Ph 4 P) 2 Se 5 and P 2 Se 5 (1 : 2), at 250 °C gave the (Ph 4 P)[In(P 2 Se 6 )] (I). Stoichiometric elemental synthesis at 750 °C produced the Cs 5 In(P 2 Se 6 ) 2 (II). The thin, yellow crystals of (I), and the irregular, dark orange cryst