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Pentavalent uranyl complexes

✍ Scribed by Polly L. Arnold; Jason B. Love; Dipti Patel

Book ID
104011046
Publisher
Elsevier Science
Year
2009
Tongue
English
Weight
459 KB
Volume
253
Category
Article
ISSN
0010-8545

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Oxo Group Protonation and Silylation of
Oxo Group Protonation and Silylation of Pentavalent Uranyl Pacman Complexes
✍ Prof. Polly L. Arnold; Anne-Frédérique Pécharman; Dr. Jason B. Love 📂 Article 📅 2011 🏛 John Wiley and Sons 🌐 English ⚖ 325 KB

## Experimental Section Synthetic procedures and characterizing data. 3: To a solution of 2 (250 mg, 0.21 mmol) in pyridine was added 1.9 equivalents of HCl in Et 2 O (2.0 mL, 0.4 mmol). The resulting suspension was stirred for 2 h, after which the precipitate was isolated and dried under vacuum,