Oxo Group Protonation and Silylation of
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Prof. Polly L. Arnold; Anne-Frédérique Pécharman; Dr. Jason B. Love
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Article
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2011
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John Wiley and Sons
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English
⚖ 325 KB
## Experimental Section Synthetic procedures and characterizing data. 3: To a solution of 2 (250 mg, 0.21 mmol) in pyridine was added 1.9 equivalents of HCl in Et 2 O (2.0 mL, 0.4 mmol). The resulting suspension was stirred for 2 h, after which the precipitate was isolated and dried under vacuum,