✦ LIBER ✦

Partial synthesis of aldosterone

✍ Scribed by W. Nagata; M. Narisada; T. Sugasawa

Publisher: Elsevier Science
Year: 1962
Tongue: French
Weight: 196 KB
Volume: 3
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)70954-3

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✦ Synopsis

SEVERAL methods of partial Irynthesia of aldo6terone cl), the moat potential mineral corticoid, preaenta a 8ynthesim of thin cyanation was applied to the fonctionated group. have been reported. 1 Thin paper . compound in which our method' of hydroonone (6) for introduction of the 18-Adrenoaterone wan converted, via its A 395 3 -dienolether , into the 17-monooxim (2), m,p. 250.5-252' (d.), [rrlz3 +159', in a yield of 7%. Beckmann rearrangement 4,5 of (2) afforded the lactam (3), m.p. 299*302O, [~rl~' +172O, am a main product. (3) was tran8formod * Angularly Substituted Polycyclic Compound8 IX.

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