Partial synthesis of [1-14C]phytanic acid
โ Scribed by A. Poulos; E. Barone; D. W. Johnson
- Book ID
- 118292635
- Publisher
- Springer-Verlag
- Year
- 1980
- Tongue
- English
- Weight
- 204 KB
- Volume
- 15
- Category
- Article
- ISSN
- 0024-4201
No coin nor oath required. For personal study only.
๐ SIMILAR VOLUMES
Dolichoic acid and [1-~4C] dolichoic acid were synthesized from polyprenol isolated from the leaves of the Ginkgo biloba. Grignard coupling with 3-bromo-2-methylpropyl bcnzyl ether afforded, after deprotection, the 3-polyprenyl-2methyl propanol. The alcohol was converted into a mesylate followed by
## Abstract The title work proceeds in five steps and 16% overall yield from sodium [1โ^14^C]acetate, which was converted by bromination followed by ethoxide displacement and reaction with phthaloyl dichloride to ethoxy[1โ^14^C]acetyl chloride. The thermal[2+2]cycloaddition of tetraethoxyethene wit
## 14 A method was developed to synthesize C-labelled n-qtkanes for use in cigarette smoke studies. Specifica],ly, n-[18-Cloctatriacontane was synthesized from 1 mCi [l-Clstearic acid in a radiochemical yield of 20%. synthesis were two consecutive alkylations yf tosylmethyl isocyanide followed by