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p-Toluenesulfonic acid/methanol: Mild reagent for the preparation of bile acid methyl esters

✍ Scribed by B. Dayal; J. Speck; E. Bagan; G.S. Tint; G. Salen


Book ID
119481466
Publisher
Elsevier Science
Year
1981
Tongue
English
Weight
159 KB
Volume
37
Category
Article
ISSN
0039-128X

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The use of microwave oven for the rapid
✍ B. Dayal; G. Salen; V. Dayal πŸ“‚ Article πŸ“… 1991 πŸ› Elsevier Science 🌐 English βš– 428 KB

An efficient and convenient procedure for the hydrolysis of bile acid methyl esters is described. This is achieved by the addition of aqueous lithium hydroxide in methanol/dioxane/tetrahydrofuran (or dimethylformamide) in the microwave oven. Under these conditions the formates as well as the acetate