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Lithium hydroxide/aqueous methanol: mild reagent for the hydrolysis of bile acid methyl esters

✍ Scribed by B. Dayal; G. Salen; B. Toome; G.S. Tint; S. Shefer; J. Padia

Book ID: 116065463
Publisher: Elsevier Science
Year: 1990
Tongue: English
Weight: 549 KB
Volume: 55
Category: Article
ISSN: 0039-128X
DOI: 10.1016/0039-128x(90)90021-3

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An efficient and convenient procedure for the hydrolysis of bile acid methyl esters is described. This is achieved by the addition of aqueous lithium hydroxide in methanol/dioxane/tetrahydrofuran (or dimethylformamide) in the microwave oven. Under these conditions the formates as well as the acetate