p-Phenylazobenzenesulfonyl Chloride—a New Reagent for Identification and Separation of Amines
✍ Scribed by WOOLFOLK, E. O.; REYNOLDS, W. E.; MASON, J. L.
- Book ID
- 127330151
- Publisher
- American Chemical Society
- Year
- 1959
- Tongue
- English
- Weight
- 759 KB
- Volume
- 24
- Category
- Article
- ISSN
- 0022-3263
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The title compound, easily prepared in two steps from vinyltrimethylsilane, is a useful reagent for the protection of primary and secondary amines as their sulfonamides, which are cleaved by fluoride ion. Sulfonamides are among the most stable of amine protecting groups.' However,
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