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Oxygen vs carbon alkylation of ethyl acetoacetate

โœ Scribed by Le Noble, William J.; Morris, H. Frank

Book ID
118188451
Publisher
American Chemical Society
Year
1969
Tongue
English
Weight
598 KB
Volume
34
Category
Article
ISSN
0022-3263

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๐Ÿ“œ SIMILAR VOLUMES

Oxygen alkylation in the ethyl acetoacet
Oxygen alkylation in the ethyl acetoacetate synthesis
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In a search for convenient preparative techniques, we have investigated the effect of solvent, halide, base, and temperature on the alkylation of the ambldent anion derived from ethyl acetoacetate. Our attention has focused on the use of dipolar aprotic solvents. A recent report (1) describing oxyge

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The alkyl group effect in the alkylations of ethyl acetoacetate in dimethyl sulfoxide
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Recent insights (1) in the remarkable solvent properties of dimethyl eulfoxida (DMSO), and our own interest in the chemistry of isopropcnyl ethers (2) led u8 to consider the poraibility of direot 0-alkylation of ethyl aoetoaoetate in that solvent. The connection i# that Kornblum'rr work (3) suggests